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Gas Chromatography-Mass Spectrometric Analysis of Isotopic Abundance of 13C, 2H, and 18O in Biofield Energy Treated p-tertiary Butylphenol (PTBP)
Natural Sciences (Analytical Chemistry, Method Development (Chemistr)
Gopal Nayak
Date of upload:
14.12.2016
Co-author:
Mahendra Kumar Trivedi, Alice Branton, Dahryn Trivedi, Parthasarathi Panda, Snehasis Jana
Abstract:
p-tert-Butyphenol (PTBP) is a phenolic monomer used in the synthesis of numerous industrially useful chemicals. The current research work aimed to evaluate the effect of the biofield energy treatment on the isotopic abundance ratios of PM+1/PM and PM+2/PM in PTBP using gas chromatography - mass spectrometry (GC-MS). The sample, PTBP was distributed into two parts - one part was designated as control PTBP and another part was considered as biofield energy treated PTBP. The biofield energy treatment was achieved through unique biofield energy transmission process by Mr. Trivedi (also known as The Trivedi Effect®). T1, T2, T3, and T4 were indicated to the different time interval analysis of the biofield treated PTBP. The GC-MS spectra of the both control and biofield treated PTBP showed the presence of molecular ion peak [M+] at m/z 150 (calculated 150.10 for C10H14O) along with eight major fragmented peaks at m/z 135, 107, 95, 91, 77, 65, 41, and 39, which might be due to C10H15+, C7H7O+ or C8H11+, C6H7O+, C7H7+, C6H5+, C5H5+, C3H5+, and C3H3••+ ions, respectively. The relative intensities of the parent molecule and other fragmented ions of the biofield treated PTBP were altered as compared to the control PTBP. The percentage in the isotopic abundance ratio of PM+1/PM was enhanced in the biofield treated PTBP at T2, T3 and T4 by 1.60%, 3.57%, and 120.13%, respectively while it was decreased by 4.14% in the treated sample at T1 with respect to the control PTBP. Consequently, the isotopic abundance ratio of PM+2/PM was increased in the biofield treated PTBP at T1, T3, and T4 by 1.28%, 2.56%, and 123.08%, respectively with respect to the control sample. On the other hand, it was reduced in the biofield treated sample at T2 by 1.28% as compared to the control PTBP. Concisely, 13C, 2H, and 17O contributions from (C10H14O)+ to m/z 151 and 18O contribution from (C10H14O)+ to m/z 152 in the biofield treated PTBP were changed with respect to the control sample and was found to have time dependent effect. The biofield energy treated PTBP might display isotope effects such as different physicochemical and thermal properties, rate of the reaction, selectivity and binding energy due to the changed isotopic abundance ratio as compared to the control sample. Biofield treated PTBP could be valuable for the designing new chemicals and pharmaceuticals through using its kinetic isotope effects.
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Metal nanoparticle field-effect transistor
Natural Sciences (Physics)
Christian Klinke
Date of upload:
20.08.2015
Co-author:
Yuxue Cai, Jan Michels, Julien Bachmann, Christian Klinke
Abstract:
We demonstrate that by means of a local top-gate current oscillations can be observed in extended, monolayered films assembled from monodisperse metal nanocrystals - realizing transistor function. The oscillations in this metal-based system are due to the occurrence of a Coulomb energy gap in the nanocrystals which is tunable via the nanocrystal size. The nanocrystal assembly by the Langmuir-Blodgett method yields homogeneous monolayered films over vast areas. The dielectric oxide layer protects the metal nanocrystal field-effect transistors from oxidation and leads to stable function for months. The transistor function can be reached due to the high monodispersity of the nanocrystals and the high super-crystallinity of the assembled films. Due to the fact that the film consists of only one monolayer of nanocrystals and all nanocrystals are simultaneously in the state of Coulomb blockade the energy levels can be influenced efficiently (limited screening). Ref: J. Appl. Phys. 114 (2013) 034311.
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Fourier Transform Infrared & Ultraviolet-Visible Spectroscopic Characterization of Ammonium Acetate & Ammonium Chloride: Impact of Biofield Treament
Natural Sciences (Analytical Chemistry, Method Development (Chemistr)
Dahryn Trivedi
Date of upload:
23.12.2016
Co-author:
Mahendra Kumar Trivedi, Alice Branton, Gopal Nayak, Khemraj Bairwa, Snehasis Jana
Abstract:
Ammonium acetate and ammonium chloride are the white crystalline solid inorganic compounds having wide application in synthesis and analytical chemistry. The aim of present study was to evaluate the impact of biofield treatment on spectral properties of inorganic salt like ammonium acetate and ammonium chloride. The study was performed in two groups of each compound i.e., control and treatment. Treatment groups were received Mr. Trivedi’s biofield treatment. Subsequently, control and treated groups were evaluated using Fourier Transform Infrared (FT-IR) and Ultraviolet-Visible (UV-Vis) spectroscopy. FT-IR spectrum of treated ammonium acetate showed the shifting in wavenumber of vibrational peaks with respect to control. Like, the N-H stretching was shifted from 3024-3586 cm-1 to 3033-3606 cm-1, C-H stretching from 2826-2893 cm-1 to 2817-2881 cm-1, C=O asymmetrical stretching from 1660-1702 cm-1 to 1680-1714 cm-1, N-H bending from 1533-1563 cm-1 to 1506-1556 cm-1 etc. Treated ammonium chloride showed the shifting in IR frequency of three distinct oscillation modes in NH4 ion i.e., at ν1, 3010 cm-1 to 3029 cm-1; ν2, 1724 cm-1 to 1741 cm-1; and ν3, 3156 cm-1 to 3124 cm-1. The N-Cl stretching was also shifted to downstream region i.e., from 710 cm-1 to 665 cm-1 in treated ammonium chloride. UV spectrum of treated ammonium acetate showed the absorbance maxima (λmax) at 258.0 nm that was shifted to 221.4 nm in treated sample. UV spectrum of control ammonium chloride exhibited two absorbance maxima (λmax) i.e., at 234.6 and 292.6 nm, which were shifted to 224.1 and 302.8 nm, respectively in treated sample. Overall, FT-IR and UV data of both compounds suggest an impact of biofield treatment on atomic level i.e., at force constant, bond strength, dipole moments and electron transition energy between two orbitals of treated compounds as compared to respective control.
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Influence of Biofield Treatment on Physicochemical Properties of Hydroxyethyl Cellulose and Hydroxypropyl Cellulose
Natural Sciences (Analytical Chemistry, Method Development (Chemistr)
Mahendra Kumar Trivedi
Date of upload:
12.07.2016
Co-author:
Gopal Nayak, Shrikant Patil, Rama Mohan Tallapragada, Rakesh Mishra
Abstract:
Cellulose based polymers have shown tremendous potential as drug delivery carrier for oral drug delivery system (DDS). Hydroxyethyl cellulose (HEC) and hydroxypropyl cellulose (HPC) are widely explored as excipients to improve the solubility of poorly water soluble drugs and to improve self-life of dosage form. This work is an attempt to modulate the physicochemical properties of these cellulose derivatives using biofield treatment. The treated HEC and HPC polymer were characterized by X-ray diffraction (XRD), differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA). The XRD studies revealed a semi-crystalline nature of both the polymers. Crystallite size was computed using Scherrer’s formula, and treated HEC polymer showed a significant increase in percentage crystallite size (835%) as compared to the control polymer. This higher increase in crystallite size might be associated with greater crystallite indices causing a reduction in amorphous regions in the polymer. However treated HPC polymer showed decrease in crystallite size by -64.05% as compared to control HPC. DSC analysis on HEC polymer revealed the presence of glass transition temperature in control and treated HEC polymer. We observed an increase in glass transition temperature in treated HEC, which might be associated with restricted segmental motion induced by biofield. Nonetheless, HPC has not showed any glass transition. And no change in melting temperature peak was observed in treated HPC (T2) however melting temperature was decreased in T1 as compared to control HPC. TGA analysis established the higher thermal stability of treated HEC and HPC. CHNSO results showed significant increase in percentage oxygen and hydrogen in HEC and HPC polymers as compared to control samples. This confirmed that biofield had induced changes in chemical nature and elemental composition of the treated polymers (HEC and HPC).
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Isotopic Abundance Analysis of Biofield Treated Benzene, Toluene and p-Xylene Using Gas Chromatography-Mass Spectrometry (GC-MS)
Natural Sciences (Analytical Chemistry, Method Development (Chemistr)
Mahendra Kumar Trivedi
Date of upload:
17.08.2016
Co-author:
Alice Branton, Dahryn Trivedi, Gopal Nayak, Gunin Saikia, Snehasis Jana
Abstract:
Benzene, toluene and p-xylene are derivatives of benzene, generally produced from crude petroleum and have numerous applications in industry. The aim of the present study was to evaluate the impact of biofield treatment on isotopic abundance of these benzene derivatives by gas chromatography-mass spectrometry (GC-MS). Benzene, toluene and p-xylene samples were divided into two parts: control and treatment. Control part was remained as untreated and treatment part was subjected to Mr. Trivedi’s biofield treatment. Control and treated samples were characterized using GC-MS. GC-MS data revealed that isotopic abundance ratio of 13C/12C or 2H/1H (PM+1/PM) of treated samples were significantly increased from un-substituted to substituted benzene rings (where, PM- primary molecule, PM+1- isotopic molecule either for 13C/12C and/or 2H/1H). The isotopic abundance ratio of 13C/12C or 2H/1H (PM+1/PM) in benzene was decreased significantly by 42.14% as compared to control. However, the isotopic abundance ratio of (PM+1/PM) in treated toluene and p-xylene was significantly increased up to 531.61% and 134.34% respectively as compared to their respective control. Thus, overall data suggest that biofield treatment has significantly altered the isotopic abundance ratio of (PM+1/PM) in a different way for un-substituted and substituted benzenes.
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Evaluation of Isotopic Abundance Ratio in Naphthalene Derivatives After Biofield Energy Treatment Using Gas Chromatography-Mass Spectrometry
Natural Sciences (Analytical Chemistry, Method Development (Chemistr)
Mahendra Kumar Trivedi
Date of upload:
17.09.2016
Co-author:
Alice Branton, Dahryn Trivedi, Gopal Nayak, Gunin Saikia, Snehasis Jana
Abstract:
Naphthalene and 2-naphthol are two naphthalene derivatives, which play important roles in the chemical and pharmaceutical industries. The aim of this study was to evaluate the impact of biofield energy treatment on the isotopic abundance of 13C/12C or 2H/1H and 18O/16O in naphthalene and 2-naphthol using gas chromatography-mass spectrometry (GC-MS). Naphthalene and 2-naphthol samples were divided into two parts: control and treated. The control group remained as untreated, while the treated group was subjected to Mr. Trivedi’s biofield energy treatment. The treated samples were subdivided into four parts named as T1, T2, T3 and T4. Control and treated samples were characterized using GC-MS. The GC-MS data revealed that the isotopic abundance ratio of 13C/12C or 2H/1H, (PM+1)/PM and 18O/16O, (PM+2)/PM were increased significantly in treated naphthalene and 2-naphthol (where PM-primary molecule, (PM+1) isotopic molecule either for 13C or 2H and (PM+2) is the isotopic molecule for 18O). The isotopic abundance ratio of (PM+1)/PM in the treated T2 samples of naphthalene and 2-naphthol was increased up to 129.40% and 165.40%, respectively as compared to their respective control. However, the isotopic abundance ratio of (PM+1)/PM in the treated T1, T3 and T4 samples of naphthalene was decreased by 44.41%, 33.49% and 30.3%, respectively as compared to their respective control. While in case of 2-naphthol, the isotopic abundance ratio of (PM+1)/PM was decreased by 39.57% in T1 sample and then gradually increased up to 9.85% from T3 to T4 samples. The isotopic abundance ratio of (PM+2)/PM in treated T2 sample of 2-naphthol was increased up to 163.24%, whereas this value was decreased by 39.57% in treated T1 sample. The GC-MS data suggest that the biofield energy treatment has significantly altered the isotopic abundance of 2H, 13C in naphthalene and 2H, 13C and 18O in 2-naphthol as compared to the control.
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An Evaluation of Biofield Treatment on Thermal, Physical and Structural Properties of Cadmium Powder
Natural Sciences (Analytical Chemistry, Method Development (Chemistr)
Gopal Nayak
Date of upload:
24.12.2016
Co-author:
Mahendra Kumar Trivedi, Shrikant Patil, Rama Mohan Tallapragada, Omprakash Latiyal, Snehasis Jana
Abstract:
Cadmium is widely utilized in nickel-cadmium batteries, stabilizers, and coating applications due to its versatile physico-chemical properties. The aim of present study was to evaluate the impact of biofield treatment on atomic, thermal, and physical properties of cadmium powder. The cadmium powder was divided into two groups, one group as control and another group as treated. The treated group received Mr. Trivedi’s biofield treatment. Control and treated samples were characterized using X-ray diffraction (XRD), differential scanning calorimetry (DSC), particle size analyzer, surface area analyzer, and scanning electron microscopy (SEM). XRD results showed significant alteration in lattice parameter, unit cell volume, densities, nuclear charge per unit volume, and atomic weight in treated cadmium powder as compared to control. Furthermore, crystallite size was significantly reduced upto 66.69% in treated cadmium as compared to control. DSC analysis results showed that the latent heat of fusion of the treated cadmium powder was considerably reduced by 16.45% as compared to control. Particle size data revealed that average particle size (d50) of treated cadmium powder was significantly reduced by 47.79 % as compared to the control. In addition, the surface area of treated cadmium powder was substantially enhanced by 156.36% as compared to control. Surface morphology observed by SEM showed the more facets and fractured surface with satellite boundaries in treated cadmium powder as compared to control. These findings suggest that biofield treatment has significantly altered the atomic, thermal and physical properties of cadmium.
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Evaluation of Thermal and Physical Properties of Magnesium Nitride Powder: Impact of Biofield Energy Treatment
Natural Sciences (Analytical Chemistry, Method Development (Chemistr)
Gopal Nayak
Date of upload:
29.11.2016
Co-author:
Mahendra Kumar Trivedi, Rama Mohan Tallapragada, Alice Branton, Dahryn Trivedi, Omprakash Latiyal, Snehasis Jana
Abstract:
Magnesium nitride (Mg3N2) has gained extensive attention due to its catalytic and optoelectronic properties. The present investigation was aimed to evaluate the effect of biofield energy treatment on physical and thermal properties of Mg3N2 powder. The Mg3N2 powder was divided into two parts i.e. control and treated. The control part was remained as untreated and the treated part was subjected to the Mr. Trivedi’s biofield energy treatment. Subsequently, the control and treated Mg3N2 samples were characterized using differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), and X-ray diffraction (XRD). The DSC results showed the specific heat capacity of 2.24 Jg-1°C-1 in control, which increased upto 5.55 Jg-1°C-1 in treated Mg3N2 sample. The TGA data revealed that the onset temperature for the formation of magnesium oxide, possibly due to oxidation of Mg3N2 in the presence of air and moisture, was reduced from 421.0°C (control) to 391.33°C in treated sample. Besides, the XRD data revealed that the lattice parameter and unit cell volume of treated Mg3N2 samples were increased by 0.20 and 0.61% respectively, as compared to the control. The shifting of all peaks toward lower Bragg angle was observed in treated sample as compared to the control. The XRD diffractogram also showed that the relative intensities of all peaks were altered in treated sample as compared to control. In addition, the density of treated Mg3N2 was reduced by 0.60% as compared to control. Furthermore, the crystallite size was significantly increased from 108.05 nm (control) to 144.04 nm in treated sample as compared to the control. Altogether data suggest that biofield energy treatment has substantially altered the physical and thermal properties of Mg3N2 powder. Thus, the biofield treatment could be applied to modulate the catalytic and optoelectronic properties of Mg3N2 for chemical and semiconductor industries.
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Evaluation of Isotopic Abundance Ratio in Biofield Energy Treated Nitrophenol Derivatives Using Gas Chromatography-Mass Spectrometry
Natural Sciences (Analytical Chemistry, Method Development (Chemistr)
Mahendra Kumar Trivedi
Date of upload:
27.07.2016
Co-author:
Alice Branton, Dahryn Trivedi, Gopal Nayak, Kalyan Kumar Sethi, Snehasis Jana
Abstract:
Nitrophenols are the synthetic organic chemicals used for the preparation of synthetic intermediates, organophosphorus pesticides, and pharmaceuticals. The objective of the present study was to evaluate the effect of biofield energy treatment on the isotopic abundance ratios of PM+1/PM, and PM+2/PM in o- and m-nitrophenol using the gas chromatography-mass spectrometry. The o- and m-nitrophenol were divided into two parts - one part was control sample, and another part was considered as biofield energy treated sample, which received Mr. Trivedi’s biofield energy treatment (The Trivedi Effect®). The biofield energy treated nitrophenols having analyzed at different time intervals were designated as T1, T2, T3, and T4. The GC-MS analysis of both the control and biofield treated samples indicated the presence of the parent molecular ion peak of o- and m-nitrophenol (C6H5NO3+) at m/z 139 along with major fragmentation peaks at m/z 122, 109, 93, 81, 65, and 39. The relative peak intensities of the fragmented ions in the biofield treated o- and m-nitrophenol were notably changed as compared to the control sample with respect to the time. The isotopic abundance ratio analysis using GC-MS revealed that the isotopic abundance ratio of PM+1/PM in the biofield energy treated o-nitrophenol at T2 and T3 was significantly increased by 14.48 and 86.49%, respectively as compared to the control sample. Consequently, the isotopic abundance ratio of PM+2/PM in the biofield energy treated sample at T2 and T3 was increased by 11.36, and 82.95%, respectively as compared to the control sample. Similarly, in m-nitrophenol, the isotopic abundance ratio of PM+1/PM in the biofield energy treated sample at T1, T3, and T4 was increased by 5.82, 5.09, and 6.40%, respectively as compared to the control sample. Subsequently, the isotopic abundance ratio of PM+2/PM at T1, T2, T3 and T4 in the biofield energy treated m-nitrophenol was increased by 6.33, 3.80, 16.46, and 16.46%, respectively as compared to the control sample. Overall, the isotopic abundance ratios of PM+1/PM (2H/1H or 13C/12C or 15N/14N or 17O/16O), and PM+2/PM (18O/16O) were altered in the biofield energy treated o- and m-nitrophenol as compared to the control increased in most of the cases. The biofield treated o- and m-nitrophenol that have improved isotopic abundance ratios might have altered the physicochemical properties and could be useful in pharmaceutical and chemical industries as an intermediate in the manufacturing of pharmaceuticals and other useful chemicals for the industrial application.
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Physical, Atomic and Thermal Properties of Biofield Treated Lithium Powder
Natural Sciences (Analytical Chemistry, Method Development (Chemistr)
Gopal Nayak
Date of upload:
22.12.2016
Co-author:
Mahendra Kumar Trivedi, Rama Mohan Tallapragada, Alice Branton, Dahryn Trivedi, Omprakash Latiyal, Snehasis Jana
Abstract:
Lithium has gained extensive attention in medical science due to mood stabilizing activity. The objective of the present study was to evaluate the impact of biofield treatment on physical, atomic, and thermal properties of lithium powder. The lithium powder was divided into two parts i.e., control and treatment. Control part was remained as untreated and treatment part received Mr. Trivedi’s biofield treatment. Subsequently, control and treated lithium powder samples were characterized using X-ray diffraction (XRD), Differential scanning calorimetry (DSC), Thermogravimetric analysis-differential thermal analysis (TGA-DTA), Scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FT-IR). XRD data showed that lattice parameter, unit cell volume, density, atomic weight, and nuclear charge per unit volume of lithium were altered after biofield treatment. The crystallite size of treated lithium was increased by 75% as compared to control. DSC analysis exhibited an increase in melting temperature of treated lithium powder upto 11.2% as compared to control. TGA-DTA analysis result showed that oxidation temperature, which found after melting point, was reduced upto 285.21°C in treated lithium as compared to control (358.96°C). Besides, SEM images of control and treated lithium samples showed the agglomerated micro particles. Moreover, FT-IR analysis data showed an alteration in absorption band (416→449 cm-1) in treated lithium sample after biofield treatment as compared to control. Overall, data suggested that biofield treatment has significantly altered the physical, atomic, and thermal properties of lithium powder.
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Physicochemical Characterization of Biofield Energy Treated Calcium Carbonate Powder
Natural Sciences (Analytical Chemistry, Method Development (Chemistr)
Gopal Nayak
Date of upload:
19.12.2016
Co-author:
Mahendra Kumar Trivedi, Rama Mohan Tallapragada, Alice Branton, Dahryn Trivedi, Omprakash Latiyal, Rakesh Kumar Mishra, Snehasis Jana
Abstract:
Calcium carbonate (CaCO3) is widely used in pharmaceutical industries and as a supplement in probiotics. The present study was designed to evaluate the effect of biofield energy treatment on the physicochemical properties of the CaCO3. The CaCO3 powder was divided into two parts and referred as control and treated. The control part was remained untreated, whereas treated part was subjected to Trivedi’s biofield treatment. The control and biofield treated samples were characterized using X-ray diffraction (XRD), particle size analyzer, surface area analyzer, thermogravimetric analysis (TGA) and Fourier transform infrared spectroscopy (FT-IR). The XRD showed that the crystallite size of treated CaCO3 was increased up to 100% as compared to the control. In addition, the lattice strain was reduced in treated sample as compared to the control. The particle size analysis result showed that the average particle size was significantly changed after treatment that led to considerably enhance the specific surface area of treated CaCO3 powder by 95% as compared to the control. The FT-IR spectroscopic analysis of the treated calcium carbonate showed shifting of wavenumber attributed to symmetric stretching vibrations of carbonate ion to higher wavenumber as compared to the control. The TGA analysis showed reduction in weight loss and increase in char yield which may be due to the increase in thermal stability of the treated sample. Therefore, the biofield treatment had significantly altered the physicochemical properties of the calcium carbonate. Hence, it is assumed that treated calcium carbonate could be used as a potential supplement of probiotics for food applications.
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The Potential Impact of Biofield Treatment on Physical, Structural and Mechanical Properties of Stainless Steel Powder
Natural Sciences (Analytical Chemistry, Method Development (Chemistr)
Gopal Nayak
Date of upload:
18.11.2016
Co-author:
Mahendra Kumar Trivedi, Shrikant Patil, Rama Mohan Tallapragada, Omprakash Latiyal, Snehasis Jana
Abstract:
Stainless steel (SS) has gained extensive attention due to its high corrosion resistance, low maintenance, familiar lustre, and superior mechanical properties. In SS, the mechanical properties are closely related with crystal structure, crystallite size, and lattice strain. The aim of present study was to evaluate the effect of biofield treatment on structural, physical and mechanical properties of SS powder. SS (Grade-SUS316L) powder was divided into two parts denoted as control and treatment. The treatment part was received Mr. Trivedi’s biofield treatment. Control and treated SS samples were characterized using particle size analyzer, X-ray diffraction (XRD), and Fourier transform infrared (FT-IR) spectroscopy. Result showed that biofield treatment has significantly reduced the particle size d10, d50, d90, and d99 (size, below which 10, 50, 90, and 99% particles were present, respectively) of SS powder up to 7.42, 12.93, 30.23, and 41.38% respectively, as compared to control. XRD result showed that the unit cell volume of SS was altered after biofield treatment. Moreover, crystallite size was significantly reduced upto 70% in treated SS as compared to control. The yield strength calculated using Hall-Petch equation, was significantly increased upto 216.5% in treated SS, as compared to control. This could be due to significant reduction of crystallite size in treated SS after biofield treatment. In FT-IR spectra, intensity of the absorption peak at wavenumber 1107 cm-1 (control) attributing to Fe-O-H bond was diminished in case of treated SS. These findings suggest that biofield treatment has substantially altered the structural, physical and mechanical properties of treated SS powder.
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